Philadelphia Paper - The Condition of Sulpher in Coal and its Relation to Coking

At the meeting of the Istitote in New York, in February, 1880," I described a process of determining sulphur iu metallic allphides, with especial reference to the determination of pyrites in coal. The procem, as then described, is as follows: A solution of sodium hydrate, of 1.25 specific gravity, is saturated with bromine. If an excess of bromiue is used it must be neutralized by the addition of a little more sodium hydrate. The pulverized mineral or coal is moistened with 25 c.e. of this solution autl heated, then hydrochloric acid is added cautiously to just acid reaction. This operation is repeated with another 25 c.c. of the alkaline solution, and again rendered acid. The mixture should be kept hot. The contents of the beaker or dish are then